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2 article(s) from Filippov, Sergey K

Synthesis and supramolecular properties of regioisomers of mononaphthylallyl derivatives of γ-cyclodextrin

Markéta Bláhová,
Sergey K. Filippov,
Lubomír Kováčik,
Jiří Horský,
Simona Hybelbauerová,
Zdenka Syrová,
Tomáš Křížek and
Jindřich Jindřich

Beilstein J. Org. Chem. 2017, 13, 2509–2520, doi:10.3762/bjoc.13.248

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Scheme 1: Preparation of 2^I-O-, 3^I-O- and 6^I-O-naphthylallyl derivatives of γ-CD by cross-metathesis.

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Scheme 2: Preparation of 2-O-, 3-O- and 6-O-NA derivatives of γ-CD by direct alkylation (see Table 1 for the yields ...

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Figure 1: Volume-weighted distribution functions for water solutions of 2-O- (2a), 3-O- (2b), and 6-O- (2c) N...

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Figure 2: Distribution functions for 2-O- (2a), 3-O- (2b), and 6-O- (2c) NA-γ-CD regioisomers in 50% MeOH (v/...

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Figure 3: Volume-weighted distribution functions for the 3-O- (2b) and 6-O- (2c) NA-γ-CD regioisomer at diffe...

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Figure 4: Effect of increasing concentration and sonication on the morphology of the 3-O-derivative 2b. A to ...

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Figure 5: Effect of increasing concentration and sonication on the morphology of the 2-O-derivative 2a. A: 2 ...

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Figure 6: Effect of increasing concentration and sonication on the morphology of the 6-O-derivative 2c. A: 0....

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Figure 7: Heat change for injection per mole of NA-γ-CD added as a function of the total concentration of NA-...

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Figure 8: ¹H NMR spectra of 2-O-derivative 2a in D₂O at concentrations of 100, 10, and 1 mM.

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Figure 9: ¹H NMR spectra of 3-O-derivative 2b in D₂O at concentrations of 100, 10, and 1 mM.

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Figure 10: Putative objects and interactions in naphthylallyl-γ-CD solution, depicted schematically for 6^I-O-n...

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Published 27 Nov 2017

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Properties of cationic monosubstituted tetraalkylammonium cyclodextrin derivatives – their stability, complexation ability in solution or when deposited on solid anionic surface

Martin Popr,
Sergey K. Filippov,
Nikolai Matushkin,
Juraj Dian and
Jindřich Jindřich

Beilstein J. Org. Chem. 2015, 11, 192–199, doi:10.3762/bjoc.11.20

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Scheme 1: Thermal decomposition of PEMEDA- and PEMPDA-β-CD with the decomposition products as characterized b...

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Figure 1: Decomposition kinetics of PEMEDA- and PEMPDA-β-CD at 50 °C as determined by ¹H NMR thermal experime...

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Scheme 2: Host and guest molecules employed in K_s determination in solution at different pH.

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Figure 2: Stability constants for β-CD with SAL, MEQ and NIA obtained by ITC measurements.

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Figure 3: Stability constants for PEMPDA-β-CD with SAL, MEQ and NIA obtained by ITC measurements.

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Scheme 3: Deposition of PEMPDA-β-CD onto solid surface (Nafion^® 117).

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Figure 4: Deposition kinetics of PEMPDA-β-CD onto Nafion^® 117 as obtained from ELSD detection of the decreasi...

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Scheme 4: Deposition of three model guests into the cavities of immobilized PEMPDA-β-CD.

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Published 02 Feb 2015

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